浩瀚色譜（山東）應(yīng)用技術(shù)開發(fā)有限公司,是齊魯大地一家從事色譜儀器技術(shù)開發(fā)，技術(shù)推廣的技術(shù)型企業(yè)，研發(fā)出多款新型產(chǎn)品。（一）專用色譜柱：1.氯乙suan直接進樣分析專用柱2.氯化氫直接進樣分析專用柱3.氯QI直接進樣分析專用柱4.四氟化硅直接進樣分析專用柱5.六氟二甲基硅醚分析專用柱6.氨氣直接進樣分析專用柱（二）痕量分析專用氣相色譜儀：1.高純氣體中痕量水（ppb級）分析專用氣相色譜儀2.純苯中痕量噻吩（ppb級）分析專用氣相色譜儀（三）防腐型氣相色譜儀，并成功應(yīng)用于氟氣，氟化氫，氯QI，氨氣，酰氯，氯化氫，三氯氫硅，四氟化硅，氯YI酸，氯HUA亞砜，硫化物，二氯化硫等腐蝕性物質(zhì)檢測，產(chǎn)品遍布各個行業(yè)及地區(qū)，其中不乏有大型央企---中石油，中儲糧，秦山核電站，中紡集團等，部分出口。

公司主要業(yè)務(wù)

1.通用氣相色譜儀生產(chǎn)銷售：氫火焰檢測器氣相色譜儀，熱導(dǎo)檢測器氣相色譜儀，火焰光度檢測器氣相色譜儀，氮磷檢測器氣相色譜儀，電子捕獲檢測器氣相色譜儀。

2.便攜式氣相色譜儀，在線氣相色譜儀生產(chǎn)銷售。

3.專用氣相色譜儀研發(fā)制造：氧化鋯檢測器氣相色譜儀，氦離子檢測器氣相色譜儀，氬離子檢測器氣相色譜儀等。

4.防腐氣相色譜儀

5.二維，多維氣相色譜儀

6.高效液相色譜儀

7.實驗室純水機，頂空進樣器，自動進樣器，熱解析儀，氮氫空發(fā)生器，色譜耗材（色譜柱，石墨墊，穩(wěn)壓閥，壓蓋鉗，頂空瓶，7725進樣閥等），分光光度計，電子天平，水分測定儀，干燥箱，離心機，玻璃儀器，化學(xué)試劑等整套實驗室設(shè)備生產(chǎn)銷售。

8.提供技術(shù)轉(zhuǎn)讓，建立分析方法。

9.從事舊色譜以舊換新的業(yè)務(wù)。

10.色譜柱研制，定做。

11.承接樣品的檢測業(yè)務(wù)。

12.承接國內(nèi)外色譜儀器的維修，改裝業(yè)務(wù)。

浩瀚色譜（山東）應(yīng)用技術(shù)開發(fā)有限公司，以客戶為中心，想客戶所想，銷售的不僅僅是產(chǎn)品，重要的是幫助客戶解決問題，架起心靈溝通的橋梁。

固定相：甲基聚硅氧烷

型號：HH-1

規(guī)格：30m*0.53mm*1.5um

近年來,隨著太陽能的不斷發(fā)展,生產(chǎn)太陽能電池的原材料—多晶硅,也隨之得到迅速發(fā)展。多晶硅的生產(chǎn)方法主要有改良西門子法、硅烷法、冶金法等。我國主要采用改良西門子法生產(chǎn)多晶硅,該方法生產(chǎn)工藝相對成熟。但核心技術(shù)仍掌握在國外發(fā)達手中,尤其是尾氣干法回收工藝,能耗高,設(shè)備維護費用高。因此,降低多晶硅生產(chǎn)過程尾氣干法回收裝置的能量消耗,具有重大的意義。

多晶硅生產(chǎn)中,干法回收氫氣作為原料還原劑和載流氣體,若其中氯hua氫含量高,則在多晶硅生產(chǎn)過程的前期可能出現(xiàn)倒?fàn)t現(xiàn)象,后期可能出現(xiàn)磷超標現(xiàn)象,嚴重影響多晶硅的質(zhì)量。因此需對回收氫氣中的氯hua氫進行測定。目前測定氯hua氫的方法有離子色譜法、分光光度法、紅外光譜法和填充柱氣相色譜法等,采用離子色譜法時需將氯hua氫轉(zhuǎn)化為Cl-進行檢測,存在操作繁瑣、耗氣量大、耗時長等缺點。

滕州市浩瀚色譜儀器技術(shù)服務(wù)有限公司，研發(fā)出《HH-1毛細管柱測定氫氣中的氯hua氫/HCL》，峰形對稱，結(jié)果滿意。

毛細管柱測定氫氣中的氯化氫 譜圖：

Determination of Hydrogen Chloride in Hydrogen by Capillary Column
Determination of Hydrogen Chloride in Hydrogen by Capillary Column Details:
Stationary phase: methyl polysiloxane
Model: HH-1
Specification: 30m*0.53mm*1.5um
In recent years, with the continuous development of solar energy, the production of polysilicon, a raw material for solar cells, has also developed rapidly. The production methods of polycrystalline silicon mainly include improved Siemens method, silane method, metallurgy method and the like. China mainly uses the modified Siemens method to produce polycrystalline silicon. The production process of this method is relatively mature. However, the core technology is still in the hands of foreign developed countries, especially the dry gas recovery process, high energy consumption and high equipment maintenance costs. Therefore, it is of great significance to reduce the energy consumption of the exhaust gas dry recovery device in the polysilicon production process.
In the production of polysilicon, the dry process recovers hydrogen as the raw material reducing agent and carrier gas. If the chlorine and hydrogen content is high, the furnace may appear in the early stage of the polysilicon production process. Phosphorus exceeding the standard may occur in the later stage, which seriously affects the quality of polysilicon. . Therefore, it is necessary to measure the chlorine hydrogen in the recovered hydrogen. At present, the methods for determining chlorohua hydrogen include ion chromatography, spectrophotometry, infrared spectroscopy and packed column gas chromatography. When ion chromatography is used, chlorohua hydrogen is converted to Cl- for detection, and the operation is cumbersome and gas-consuming. Big, long time and other shortcomings.
Tengzhou Haohao Chromatography Instrument Technology Service Co., Ltd. developed the "HH-1 capillary column for the determination of chlorohua hydrogen/HCL in hydrogen". The peak shape is symmetrical and the results are satisfactory.

Determination of Hydrogen Chloride in Hydrogen by Capillary Column: